By J S Brimacombe
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Extra resources for Carbohydrate Chemistry Volume 10
Koroteev, Z . K. Zhane, and A. A. , 1976, 47, 221. C. L. Coulter, J. Amer. Chem. , 1976, 98, 4997. Carbohydrate Chemistry 42 The preparation of carbohydrate enol phosphates, using the Perkow and o f uridine 2’,3’-(adamant-l-yl)phosphonates 237 are dealt with in Chapters 18 and 21, respectively. 2) h y d r a ~ i n e . g. tetrahydropyranyl) group in the synthesis of oligoribonucleotides by the phosphotriester approach has been Mild alkaline hydrolysis of 5’-ester protecting groups lead to cyclization of the intermediate 5’-hydroxy derivatives with the formation of dinucleoside 3’,5’-cyclic phosphates (Scheme 21).
T. Gilham, Biochemistry, 1976, 15, 4623. 5. H. van Boom, P. M. J. Burgers, P. H. van Deursen, 5. F. M. de Rooy, and C. B. S. Chem. ,1976, 167. K. K. Ogilvie, S. L. Beaucage, and D. W. Entwistle, Tetrahedron Letters, 1976, 1255. 1 M-NaOH in aqueous dioxan Scheme 21 commonly used in nucleotide phosphotriester syntheses, were rapidly removed at room temperature, and tetrabutylammonium fluoride in T H F containing glacial acetic acid could be used to remove an 0’-alkylsilyl protecting group in the presence of 2,2,2-trichloroethyl or phenyl groups.
F. L. Weitl, M. Sovak, and M. Ohno, J . Medicin. , 1976, 19, 353. F. L. Weitl, M. Sovak, T. M. Williams, and J. H. Lang, J . Medicin. , 1976, 19, 1359. L. A. Carpino, H. Ringsdorf, and H. Ritter, Makromol. , 1976, 177, 1631. K. L. Matta and J. J. , 1976, 48, 65. H. G. Garg and R. W. , 1976, 49, 482. S. C. Chhabra, S. R. Gupta, C. S. Sharma, and N. D. Sharma, Indian J. , 1976, 14B, 384 (Chem. , 1976, 85, 193 025y). L. Farkas and J. Strelisky, in ‘Topics in Flavonoid Chemistry and Biochemistry’, Proceedings of the 4th Hungarian Bioflavonoid Symposium, 1973 (Pub.
Carbohydrate Chemistry Volume 10 by J S Brimacombe